Broad spectrum sunscreen lotion from Hallstar.
Broad Spectrum SPF 50 Sunscreen Lotion
The HallStar Company
(877) 427-4255, (312) 385-4494 * www.hallstar.com
E-mail: customerservice@hallstar.com
INGREDIENTS: % WT.
Phase A
Water (deionized) 49.110
Versene NA (Dow Chemical) (Disodium EDTA) 0.100
Rhodicare XC (Rhodia) (Xanthan gum) 0.200
Phase B
Parsol MCX (DSM Nutritional) (Ethylhexyl methoxy- 7.500
cinnamate [octinoxate])
X-Tend 226 (ISP) (Phenethyl benzoate) 5.000
HallStar GC (HallStar) (Caprylic/capric 3.750
triglyceride)
SolaStay S1 (HallStar) (Ethylhexyl methoxycrylene) 6.000
Phase C
Parsol 1789 (DSM Nutritional) (Butyl methoxy- 3.000
dibenzoylmethane [avobenzone])
Phase D
Ganex V-220 (ISP) (VP/eicosene copolymer) 1.000
Novel II TDA-12 ethoxylate (Sasol) (Trideceth-12) 1.000
Ceralution H (Sasol) (Behenyl alcohol (and) 1.000
glyceryl stearate (and) glyceryl stearate citrate
(and) disodium ethylene dicocamide PEG-15
disulfate)
Phase E
Water (deionized) 11.047
Sodium hydroxide NF (General Chemical) 0.200
(Sodium hydroxide)
Neo Heliopan Hydro (Symrise) 2.000
(Phenylbenzimidazole sulfonic acid [ensulizole])
Sodium hydroxide NF (General Chemical) 0.093
(Sodium hydroxide)
Phase F
Benzyl alcohol, ACS, 99+% (Alfa Aesar) 1.000
(Benzyl alcohol)
Superol K, glycerine 99.7% USP/FCC Kosher 4.000
(P&G Chemicals) (Glycerin)
CoSept M (HallStar) (Methylparaben) 0.100
CoSept E (HallStar) (Ethylparaben) 0.050
Phase G
Ceralution F (Sasol) (Disodium ethylene dicocamide 1.000
PEG-15 disulfate (and) sodium lauroyl lactylate)
Phase H
Sodium hydroxide NF (General Chemical) 0.350
(Sodium hydroxide [20% aq])
Phase I
Simulgel 600 (Seppic) (Acrylamide/sodium 2.500
acryloyldi-methyltaurate copolymer (and)
isohexadecane (and) polysorbate 80)
PROCEDURE: Prepare phase A by adding EDTA to water and when
dissolved adding xanthan gum and mixing until fully incorporated.
In a separate vessel combine phase B, start heating with mixing to
75[degrees]C, add phase C and when completed dissolved add phase D
in order. In another vessel combine phase E, in order, using only
enough sodium hydroxide to achieve complete solution (pH 7.5-8.0).
In another vessel combine phase F and mix until a clear solution.
Transfer slightly less than half of A to the empty main vessel, add
phase G, and then heat to 65[degrees]C. With both phases at
indicated temperatures, add phase BCD to phase AG with mixing and
then start homogenizing. After five minutes, add F to ABCDG, then
add the remainder of phase A, and then add phase E. Switch from
homogenization to mixing, adjust pH to 75-8.0 with phase H as
needed, and start cooling. Add phase I with sweep mixing (to
prevent aeration) and then add water as needed to correct for
evaporative losses. When completely smooth, perform final quality
assurance checks. PROPERTIES: Light yellow lotion; pH: 7.75;
Viscosity (RV, T-D, 5, 20 & 100 rpm, cP): 6000, 2300 & 900.
COMMENTS: SolaStay $1, a novel sunscreen photostabilizer, quenches
the singlet excited states of octinoxate and avobenzone to provide
superior SPF and PFA performance. U.S. patents pending. This
formula yields superior broad-spectrum protection with daily
wear-appropriate aesthetics. SolaStay $1, a novel sunscreen
photostabilizer, quenches the singlet excited states of octinoxate
and avobenzone. It provides superior SPF and PFA performance by
contributing to their photostability in this formula, resulting in
in vivo SPF 50.80 and PFA (PPD) 19.36 test results in five subject
static testing on the reference formula.
Clear Water-Resistant Hair Gel
Lubrizol Advanced Materials Inc. (Noveon Consumer Specialties)
(216) 447-5000, (800) 379-5389 * www.personalcare.noveon.com
INGREDIENTS: % WT.
Phase A
Deionized water 71.83
Butylene glycol (Merck) 1,3-butanediol 3.00
AMP-Ultra PC 2000 (95%) (Dow/Angus) 0.05
(Aminomethyl propanol)
Avalure AC 120 acrylic copolymer (29% TS) 3.50
(Lubrizol/Noveon) (Acrylates copolymer)
Fixate Plus Polymer (30% TS) (Lubrizol/Noveon) 10.00
(Polyacrylate-14)
AMP-Ultra PC 2000 (Dow/Angus) (95%) 0.46
(Aminomethyl propanol)
Glydant Plus Liquid (Lonza) (DMDM hydantoin (and) 0.50
iodopropynyl butylcarbamate)
Ethanol absolute (VWR) (Alcohol) 10.00
Vitalmixt BDF # 143149 (Symrise) (Fragrance) 0.10
AMP-Ultra PC 2000 (95%) (Dow/Angus) 0.56
(Aminomethyl propanol)
PROCEDURE: Add deionized water and butylene glycol in a suitable
vessel. Start mixing. Adjust the pH of batch to ~10 by adding a few
drops of AMP-Ultra PC 2000 into the batch. Slowly add Avalure AC
120 acrylic copolymer to the batch. Mix for 5 minutes. Slowly add
Fixate Plus polymer to the mixing vessel. Mix for 5 minutes or
until uniform. Pre-neutralize the batch with AMP-Ultra PC 2000,
adjusting pH to 5.5-6.0. In a separate level, mix Glydant Plus
Liquid, ethanol and fragrance. Mix until homogenous. Add it slowly
to the batch. Mix until homogenous. Adjust final pH to 7.0-7.2 with
AMP-Ultra PC 2000. Mix until uniform. PROPERTIES: Appearance--Clear
gel; pH--7.0-7.2; Viscosity (mPa.s) (Brookfield DV-II+Pro
Viscometer @ 20 rpm, 25[degrees]C, # spindle, measured after 24
hours)--45,000-50,000; Turbidity (NTU) (HF Scientific Micro 100
Turbidimeter)--10-20; Water/sweat immersion resistance--90%; (1.85
g of hair gel is applied on clean Virgin European Brown tresses
(0.74g of gel per gram of hair). Treated tresses are wrapped on
5/8" diameter plastic smooth barrel hair curlers, 2" in length and
allowed to dry overnight (50% RH-23[degrees]C). Dried, treated
tresses are gently removed from the rollers and submerged in a
sweat salts water bath for 3 minutes, and measurements recorded at
1 minute intervals for 3 minutes) Stability--passed 3 months @ 45
[degrees]C, 5 cycles freeze/thaw. COMMENTS: Due to the alcohol in
this formulation, it is recommended that customers review the
environmental and regulatory requirements of the states and
countries where they wish to market this type of product to be sure
that they are in compliance with local VOC regulations. Due to the
alcohol in this formulation, follow safety precautions appropriate
for the handling of flammable liquids.
Hair Wax Stick
Natunola Health, Inc.
(613) 774-9998 x www.natunola.com
E-mail: admin@natunola.com
INGREDIENTS: % WT.
Phase A
Natunola canola oil (Natunola Health Inc.) q.s.
Vegelatum Clear RM (Natunola Health Inc.) 25.0
Natunola Castor 1023 (Natunola Health Inc.) 1.0
Aloe vera oil gel C1XW (Natunola Health Inc.) 4.0
Candelilla wax (Ross Waxes) 9.0
Stearyl alcohol (Croda) 16.0
Cetyl alcohol (Ashland) 14.0
Dimethicone (Dow) 1.0
Color, fragrance q.s.
PROCEDURE: Heat all ingredients to 80-85[degrees]C with rapid
stirring to disperse gels. Cool to 65-70[degrees]C to fill.
Rinse-Off Conditioner for Unruly Hair
Dow Corning Corporation
Tel: (989) 496-6000; lifesciences@dowcorning.com
www.dowcorning.com/content/personal/
INGREDIENTS: % WT.
Phase A
Distilled water 50.0
Natrolsol 250 HHR (Hercules Inc.) 1.5
(Hydroxyethyl cellulose)
Arquad 16-29(Akzo Nobel Chemicals Inc.) 0.3
(Cetrimonium chloride)
Phase B
Lanette O (Cognis) (Cetearyl alcohol) 1.0
Arlacel 165 (Croda Inc.) (Glyceryl stearate 1.0
(and) PEG-100 stearate)
Dow Corning 2-8566 Fluid (Amodimethicone) 2.0
Phase C
Distilled water to 100.0
Phase D
Preservative (choice) 0.2
PROCEDURE: Heat water of phase A to about 75[degrees]C and add
remaining ingredients, mixing until uniform. Using a water bath,
combine phase B ingredients and mix until temperature reaches
60-70[degrees]C. Heat phase C to 80[degrees]C. Add phase C to phase
B, mixing at high speed for 10 minutes. Add BC to phase A, mixing
gently until uniform. Cool to room temperature with gentle mixing.
Add phase D. COMMENTS: This rinse-off conditioner provides
long-lasting conditioning without buildup. It enhances wet and dry
combing and smoothes unruly hair, while improving color depth and
longevity.
Soft Skin Facial Cream with Stratagel 500
Centerchem, Inc.
(203) 822-9800 * www.centerchem.com
INGREDIENTS: % WT.
Phase A
Deionized water 67.85
Ultrez 10 (Lubrizol) (carbomer) 0.20
Hispagel oil LV (Cognis/Centerchem) 10.00
Phase B
Promulgen D (Lubrizol) (Cetearyl alcohol and 2.00
ceteareth-20)
Cutina GMS-SE (Cognis) (Glyceryl stearate) 1.25
Myrj 59 (Unigema) (PEG-100 stearate) 1.00
Tegosoft CT (Evonik) (Capric/caprylic triglyceride) 2.00
Stratagel 500 (Centerchem) 15.00
Phase C
Sodium hydroxide (10% solution) q.s.to pH 6.5-7
Phase D
Diocide (Lipotec/Centerchem) 0.70
PROCEDURE: Disperse carbomer in water, mix until uniform. Add
remaining phase A ingredients, heat to 80[degrees]C. Heat phase B
to 80[degrees]C. Add phase B to phase A under moderate mixing. Mix
for 5 minutes, then homogenize until uniform. Begin cool down. At
50[degrees]C, add phase C until batch is between pH 6.5-7.0 At
40[degrees]C, add phase D. Mix until uniform. Discontinue.
Hand Cleanser
DuPont Tate & Lyle Bio Products
(866) 404-7933 (U.S., Canada & Mexico); (217) 421-3443
www.duponttateandlyle.com
INGREDIENTS: % WT.
Phase A
Ammonium lauryl sulfate (ALS) (28%) 26.0
Cocamide DEA 6.0
Sodium lauryl sulfate (SLS) (25%) 18.0
Zemea propanediol (Dupont Tate & Lyle) 2.0
Water 44.5
Zemea stearate (Dupont Tate & Lyle) 0.5
Irgasan 0.2
Tetrasodium EDTA (5 wt.%) 2.0
Fragrance q.s.
Citric acid (50 wt.%) q.s.
PROCEDURE: Blend ALS, cocamide DEA, SLS and Zemea propanediol. Add
Zemea stearate. Heat to 60[degrees]C. Cool to 30[degrees]C. Add
Irgasan and EDTA. Stir until homogeneous solution is formed. Adjust
to pH 6 with citric acid. Add fragrance.
Extra Moisturizing Acne Treatment Night Cream
Air Products & Chemicals Personal Care
(610) 481-6799 x www.airproducts.com/personalcare
INGREDIENTS: % WT.
Phase A
Deionized water 67.6
Keltrol CG-T (CP Kelco) 0.25
Pemulen TR-2 (Lubrizol) (Acrylates/C10-30 alkyl 0.25
acrylate cross polymer)
Propylene glycol (RITA) 2.0
Butylene glycol (Ruger) 1.0
Hexylene glycol (Ruger) 1.0
Salicylic acid powder 2.0
Intelimer 8600 (Air Products) 2.2
(Poly C8-22 Alkyl acrylate/metacrylic acid cross polymer)
Allantoin (DSM) 0.5
Natural alpha bisabolol 0.15
Phase B
Finsolv TN (Innospec) (C12-15 alkyl benzoate) 3.0
Crodacol C-95 (Croda) (Cetyl alcohol) 5.5
Dow Corning 200/100 (Dow Corning) (Dimethicone) 5.6
Natural Beeswax (RITA) 2.5
Amphisol K (DSM) (Potassium cetyl phosphate) 1.0
Glyceryl stearate 2.0
Hydrogenated castor oil 1.0
Arlacel 165 (Croda) (PEG-100 stearate) 1.5
Cetiol LC (Cognis) (Coco caprylate/caprate) 1.0
PROCEDURE: Combine all phase A ingredients into a vessel while
stirring mixture. In another vessel add deionized water then slowly
add xanthan gum and salicylic acid while stirring. Continue to stir
until clear homogenous mixture forms. Add other remaining phase B
ingredients one by one to the gum and acid mixture while continuing
to stir. Begin heating both vessels until the temperature of both
vessels is between 80-85[degrees]C. Once at 80-85[degrees]C
temperature has been achieved add phase A to phase B slowly while
continuing to stir the mixture. Remove from heat and homogenize the
resulting mixture for three minutes. Let the emulsion cool to the
desired temperature. Adjust the pH with a few drops of
triethanolamine (TEA 99%) and package.
Daily Pep Cream
Evonik Goldschmidt
(49) 201-173-2854 x www.evonik.com/personal-care
Email: personal-care@evonik.com
INGREDIENTS: % WT.
Phase A
Abil EM 90 (Cetyl PEG/PPG-10/1 dimethicone) 2.0
Isolan GI 34 (Polyglyceryl-4 isostearate) 1.0
Hydrogenated castor oil 0.8
Paracera W 80 (Paramelt B.V.) (Microcrystalline wax) 1.2
Isohexadecane 9.5
Tegosoft CT (Evonik) (Caprylic/capric triglyceride) 6.5
Tegosoft liquid (Evonik) (Cetearyl ethylhexanoate) 4.0
Phase B
Tego Pep 4-17 (Evonik) (Tetrapeptide-21; glycerin; 2.0
butylene glycol; aqua)
Sodium chloride 0.5
Water 72.5
Phase Z
Preservative, perfume q.s.
PROCEDURE: Heat phase A to approximately 80[degrees]C. Add phase B
(80[degrees]C or room temperature) slowly while stirring.
Homogenize for a short time. Cool with gentle stirring below
30[degrees]C and homogenize again.
Rich Hair Conditioning Shampoo
Cognis GmbH, Care Chemicals Division
Monheim, Germany * www.cognis.com
Phase A
Water, demineralized 75.85
Jaguar C 17 (Rhodia) (Guar hydroxypropyltrimonium 0.2
chloride)
Phase B
Texapon N 70 (Cognis) (Sodium laureth sulfate) 14.3
Dehyton PK 45 (Cognis) (Cocamidopropyl betaine) 5.4
Dehydol LS 2 Deo N (Cognis) (Laureth-2) 1.0
Lamesoft Care (Cognis) (PEG-4 distearyl ether (and) 2.0
sodium laureth sulfate (and) distearyl ether (and)
dicaprylyl ether)
Perfume, preservative q.s.
Sodium chloride 0.75
Citric acid (50%) 0.50
PROCEDURE: Introduce water and disperse Jaguar C 17 at room
temperature while stirring. Add ingredients of phase B in given
order under mixing until homogeneous. Adjust pH value with citric
acid and viscosity with sodium chloride. The amount of citric acid
and sodium chloride is approximate. PROPERTIES: pH-value (as is):
~5.5; Viscosity (Brookfield RVT, 23[degrees]C, spindle 4, 10 rpm):
~7400 mPas; Density (g/cm3): ~1.0350
COPYRIGHT 2009 Rodman Publishing
No portion of this article can be reproduced without the express written permission from the copyright holder.
Copyright 2009 Gale, Cengage Learning. All rights reserved.
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